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OSUMethods and References
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Soil Analysis pH Thomas, G.W. 1996. Soil pH and soil acidity. p. 475-490. In: Methods of Soil Analysis, Part 3—Chemical Methods. Soil Science Society of America, Madison, WI, USA. Watson, M. E. and J.R. Brown. 1998. pH and Lime Requirement, p. 13-16. In: Recommended Chemical Soil Test Procedures for the North Central Region. NCR Publication No. 221. Missouri Agricultural Experiment Station, Columbia, MO, USA.
Lime Test Index Sims, J. T. 1996. Lime Requirement. p. 491-515. In: Methods of Soil Analysis, Part 3—Chemical Methods. Soil Science Society of America, Madison, WI, USA. Watson, M. E. and J.R. Brown. 1998. pH and Lime
Requirement, p. 13-16. In: Recommended Chemical Soil Test Procedures for the
North Central Region. NCR Publication No. 221. Missouri Agricultural Experiment
Station, Columbia, MO, USA. Soil Bray P1 Extraction Kuo, S. 1996. Phosphorus. p. 894-895. In: Methods of Soil Analysis, Part 3—Chemical Methods. Soil Science Society of America, Madison, WI, USA. Frank, K, D. Beegle and J. Denning. 1998. Phosphorus, p. 21-23. In: Recommended Chemical Soil Test Procedures for the North Central Region. NCR Publication No. 221. Missouri Agricultural Experiment Station, Columbia, MO, USA.
Exchangeable Ca, Mg, K, Na – One Molar (1 M) Ammonium Acetate Extraction Warncke, D. and J.R. Brown. 1998. Potassium and other basic cations, p. 31-33. In: Recommended Chemical Soil Test Procedures for the North Central Region. NCR Publication No. 221. Missouri Agricultural Experiment Station, Columbia, MO, USA. Helmke, P. A. and D. L. Sparks. 1996. Lithium, sodium, potassium, rubidium, and cesium. p. 568-569. In: Methods of Soil Analysis, Part 3—Chemical Methods. Soil Science Society of America, Madison, WI, USA.
Extractable P, K, Ca, Mg, Mn, Cu and Zn - Mehlich 3 Extraction Mehlich, A 1984. Mehlich 3 soil test extractant: A modification of Mehlich 2 extractant. Communications in Soil Science and Plant Analyses 15:1409-1416. Helmke, P. A. and D. L. Sparks. 1996. Lithium, sodium, potassium, rubidium, and cesium. p. 567-568. In: Methods of Soil Analysis, Part 3—Chemical Methods. Soil Science Society of America, Madison, WI, USA.
Electrical Conductivity and Soluble Salts Whitney, D.A. 1998. Soil salinity. p. 59-60. In: Recommended Chemical Soil Test Procedures for the North Central Region. NCR Publication No. 221. Missouri Agricultural Experiment Station, Columbia, MO, USA. Jackson, M.L. 1958. Soil Chemical Analysis. Prentice-Hall, Englewood Cliffs, NJ, USA. Rhoades, J. D. 1996. Salinity: Electrical conductivity and total dissolved solids. p. 417-435. In: Methods of Soil Analysis, Part 3—Chemical Methods. Soil Science Society of America, Madison, WI, USA.
Nitrate - Nitrogen Gelderman, R.H. and D. Beegle 1998. Nitrate-nitrogen. p. 17-20. In: Recommended Chemical Soil Test Procedures for the North Central Region. NCR Publication No. 221. Missouri Agricultural Experiment Station, Columbia, MO, USA. Mulvaney, R.L. 1996. Nitrogen - inorganic forms. p. 1162-1171. In: Methods of Soil Analysis, Part 3—Chemical Methods. Soil Science Society of America, Madison, WI, USA.
Inorganic Nitrogen – Two Molar (2 M) KCl Extraction Mulvaney, R.L. 1996. Nitrogen - inorganic forms. p. 1129-1139. Methods of Soil Analysis, Part 3—Chemical Methods. Soil Science Society of America, Madison, WI, USA. Gelderman, R.H. and D. Beegle. 1998. Nitrate-Nitrogen, p. 17-18. In: Recommended Chemical Soil Test Procedures for the North Central Region. NCR Publication No. 221. Missouri Agricultural Experiment Station. Columbia, MO, USA.
Exchangeable Aluminum – One Molar (1 M) KCl Extraction Bertsch, P.M. and P.R. Bloom. 1996. Aluminum. p. 526-527. In: Methods of Soil Analysis, Part 3—Chemical Methods. Soil Science Society of America, Madison, WI, USA.
Boron - Hot Water Soluble Keren, R. 1996. Boron. p. 610-611. In: Methods of Soil Analysis, Part 3—Chemical Methods. Soil Science Society of America, Madison, WI, USA.
Total Concentrations of Elements - Digestion with HClO4/HNO3 Followed by Inductively Coupled Plasma (ICP) Emission Spectrometry Sommers, L. E. and D. W. Nelson. 1972. Determination of Total Phosphorus in Soils: A Rapid Perchloric Acid Digestion Procedure. Soil Science Society of America Proceedings. Vol. 36, 6: p.902-904. Madison, WI. Jackson, M.L. 1958. Soil Chemical Analysis. Prentice-Hall, Englewood Cliffs, NJ, USA. Hossner, L.R. 1996. Dissolution for total elemental analysis. p. 49-64. In: Methods of Soil Analysis, Part 3—Chemical Methods. Soil Science Society of America, Madison, WI, USA.
Ammonia - Nitrogen Mulvaney, R.L. 1996. Nitrogen - inorganic forms. p. 1129-1139. In: Methods of Soil Analysis, Part 3—Chemical Methods. Soil Science Society of America, Madison, WI, USA.
Total Nitrogen AOAC Official Methods of Analysis. Method 990.03. Protein(crude) in Animal Feed Combustion Method(Dumas method). 17th edition 2002. Reference: JAOAC 72, 770(1989)
Organic Matter / Loss on Ignition Combs, S. M. and M. V. Nathan 1998. Soil organic matter. p. 53-58. In: Recommended Chemical Soil Test Procedures for the North Central Region. NCR Publication No. 221. Missouri Agricultural Experiment Station, Columbia, MO, USA.
Total Carbon International Standard, ISO 10694:1995(E). Soil quality – Determination of organic and total carbon after dry combustion (elementary analysis). International Organization for Standardization. Geneva, Switzerland.
Inorganic Carbon US EPA Test Methods for Evaluating Solid Wastes. Chapter 5 Miscellaneous Test Methods. Methods 9060A: Total Organic Carbon. SW-846. 3rd edition. Electrical Conductivity and Soluble Salts Jackson, M.L. 1958. Soil Chemical Analysis. Prentice-Hall, Englewood Cliffs, NJ, USA. Rhoades, J. D. 1996. Salinity: Electrical conductivity and total dissolved solids. p. 417-435. In: Methods of Soil Analysis, Part 3—Chemical Methods. Soil Science Society of America, Madison, WI, USA.
Nitrate-Nitrogen Mulvaney, R.L. 1996. Nitrogen - inorganic forms. p. 1162-1171. In: Methods of Soil Analysis, Part 3—Chemical Methods. Soil Science Society of America, Madison, WI, USA. Gelderman, R.H. and D. Beegle 1998. Nitrate-nitrogen. p. 17-20. In: Recommended Chemical Soil Test Procedures for the North Central Region. NCR Publication No. 221. Missouri Agricultural Experiment Station, Columbia, MO, USA.
Percent Moisture Percent Ash
Total Concentrations of Elements - Digestion with HClO4/HNO3 Followed by Inductively Coupled Plasma (ICP) Emission Spectrometry AOAC Official Method 975.03 Metals in Plants and Pet Foods Atomic Absorption Spectrophotometric Method, First Action 1975, Final Action 1988 Allen, J.E. 1971. Preparation of Agricultural Samples for Analysis by Atomic Absorption Spectroscopy. Ruakura Soil Research Sta., Hamilton, New Zealand. Isaac, R.A. and W.A. Johnson. 1985. Elemental Analysis of Plant Tissue by Plasma Emission Spectroscopy: Collaborative Study. J. Assoc. Off. Anal. Chem.(Vol.68, No. 3. P499, 1985). Johnston, C.M. and Ulrich. 1959. Analytical Methods for use in Plant Analysis.California Agricultural Exp. Sta. Bulletin #766.
Total Concentrations of Elements – Microwave Digestion with HNO3 Followed by Inductively Coupled Plasma (ICP) Emission Spectrometry Jones, J. B. Sr., B. Wolf and H. A. Mills. 1991. Microwave Digestion Using CEM Microwave Digestion System. In: Plant Analysis Handbook. Micro-Macro Publishing. Athens, GA. Isaac, R.A. and W.A. Johnson. 1985. Elemental analysis of plant tissue by plasma emission spectroscopy: Collaborative study. Journal of Association of Official Analytical Chemists 68:499-505.
Total Nitrogen (Combustion Analysis) AOAC Official Methods of Analysis. Method 990.03.
Protein(crude) in Animal Feed Combustion Method(Dumas method). 17th edition
2002. Reference: JAOAC 72, 770(1989) Nitrate-Nitrogen Baker, A.S. and R. Smith 1969. Extracting Solution for Potentiometric Determination of Nitrate in Plant Tissue. J. Agr. Food Chem. 17: 1284 - 1287. Chloride LaCroix, R.L.,D. R. Keeney and L. M. Walsh, 1970. Potentiometric Titration of Chloride in Plant Tissue Extracts using the Chloride Ion Electrode. Soil Sci. and Plant Analysis, 1(1), p.1– 6. Johnston, C.M. and Ulrich. 1959. Analytical Methods for use in Plant Analysis.California Agricultural Exp. Sta. Bulletin #766, p39 – 41. LeGrys VA, Basrfitt MF, Gibson LE, Hammond RB, Kraft K.. National Committee for Clinical Laboratory Standards (NCCLS) Sweat Testing: Sample Collection and Quantitative Analysis; Approved Guideline. NCCLS document C34-A2, Vol. 20 No. 14 (ISBN 1-56238-407-4) NCCLS, Pennsylvania
Fiber Analysis Van Soest, P. J., 1963. Use of detergents in the analysis of fibrous feeds. II. A rapid method for the determination of fiber and lignin. J.A.O.A.C. 46:829 - 35. Goering, H. K. and P. J. Van Soest. Forage Fiber Analysis
(Apparatus, Reagents, Procedures, and some Applications). Agricultural handbook
379, U.S. Department of Agriculture.
Total Sulfur Sulfur Analyzer (dry combustion) – Analytical Instruments for Plant Analysis. M. E. Watson and R. A. Isaac, Chapter 26. In: Soil testing and Plant Analysis, 3rd Edition, Soil Science Society of America, Madison WI.
Standard Test
Method for Sulfur in Ash from Coal, Coke, and Residues from Coal Combustion
Using High-Temperature Tube Furnace Combustion Method with Infrared Absorption
Compost and Biosolids Analysis Test Methods for the Examination of Composting and Compost (TMECC). 2002, US Composting Council Research and Education Foundation. Holbrook, NY TMECC methods are the basis for all compost analysis. Percent Solids 03.09-A Total Solids and Moisture at 70C % Ash / Votalile Solids 03.02-A Unmilled Material Ignited at 550C without Inerts Removal pH 04.11-A 1:5 Slurry Method, Mass Basis Soluble Salts / Electrical Conductance 04.10-A 1:5 Slurry Method, Mass Basis Total Nitrogen 04.02-D Total Nitrogen by Oxidation, Dumas Method Nitrate- Nitrogen 04.02-B Nitrate by Ion Chromatography Ammonium Nitrogen Micro-Kjeldahl distillation of wet sample Total Carbon 04.01-A Combustion with CO2 Detection Total Mineral Analysis 04.12-A Microwave-Assisted Nitric Acid Digestion, US EPA 3051, Plus ICP analysis
MANURE ANALYSES Recommended
Methods of Manure Analysis -- University of Wisconsin-Madison,
Editor: John Peters Water Acidity -- Section 2310 Alkalinity -- Section 2320 Conductivity -- Section 2350 Residue of Evaporation -- Section 2540 Total Dissolved Solids - 180C Anions by Ion Chromatography -- Section 4110C. Single-Column Ion Chromatography with Electronic Suppression of Eluent Conductivity and Conductimetric Detection. Metals by ICP -- Section 3120B. Metals by Plasma Emission Spectroscopy. Greenberg, A.E., L.S. Clesceri and A.D. Eaton. 1992. In: Standard Methods for the Examination of Water and Wastewater, 18th ed. American Public Health Association, American Water Works Association and Water Environment Federation. APHA-AWWA-WEF, Washington, DC
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